(C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)

Base Information

Chemical Name:(C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)
CAS No.:149538-46-5
Molecular Formula:C₂₄H₂₁N₃OSSn
Molecular Weight:518.226
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)3Sn(C<sub>4</sub>H<sub>3</sub>OCHNNCSNH<sub>2</sub>)

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Chemical Property of (C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)

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Technology Process of (C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)

There total 2 articles about (C₆H₅)3Sn(C₄H₃OCHNNCSNH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 5419-96-5,153750-93-7
furan-2-aldehyde thiosemicarbazone

: 639-58-7
triphenyltin chloride

: 149538-46-5
(C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)

Guidance literature:: With sodium; In methanol; benzene; byproducts: NaCl; addn. of Na to a soln. of ligand in a dry solvent mixt. (benzene/MeOH, in the absence of moisture), addn. of mixt. to a soln. of Ph3SnCl in benzene/MeOH, refluxing for 12-14 h; filtration, refluxing again, filtration (removing NaCl), removing solvent by distn. under reduced pressure, washing repeatedly with dry n-hexane and petroleum ether, drying in vacuo under reduced pressure, elem. anal.;

Reference yield: 64.0%

: 5419-96-5
furfuraldehyde thiosemicarbazone

: 639-58-7
triphenyltin chloride

: 149538-46-5
(C₆H₅)3Sn(C₄H₃OCHNNCSNH₂)

Guidance literature:: With NaOCH₃; In methanol; benzene; byproducts: NaCl; dropwise addn. of ligand in abs. MeOH/C6H6 (3:1) to NaOCH3 soln. (under N2); stirring 1h; addn. of Ph3SnCl in MeOH; stirring 1h; refluxing 3-4h; cooling; centrifugation; concg. clear soln. by distn.; pptn.; filtration; recrystn. (MeOH); drying in vac. (P2O5); elem. anal.;