Technology Process of C24H31NO12
There total 6 articles about C24H31NO12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / acetonitrile / 0.04 h / 40 - 60 °C / Microwave irradiation
2: citric acid / tetrahydrofuran; water / 2 h
With
boron trifluoride diethyl etherate; citric acid;
In
tetrahydrofuran; water; acetonitrile;
1: Helferich method;
DOI:10.1080/07328303.2010.508295
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / acetonitrile / 0.03 h / 40 - 60 °C / Microwave irradiation
2: citric acid / tetrahydrofuran; water / 2 h
With
boron trifluoride diethyl etherate; citric acid;
In
tetrahydrofuran; water; acetonitrile;
1: Helferich method;
DOI:10.1080/07328303.2010.508295
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / benzene / 12 h / Reflux; Dean-Stark apparatus
1.2: 1.5 h / 0 °C
2.1: acetonitrile / 16 h / 20 °C
3.1: boron trifluoride diethyl etherate / acetonitrile / 0.03 h / 40 - 60 °C / Microwave irradiation
4.1: citric acid / tetrahydrofuran; water / 2 h
With
boron trifluoride diethyl etherate; toluene-4-sulfonic acid; citric acid;
In
tetrahydrofuran; water; acetonitrile; benzene;
3.1: Helferich method;
DOI:10.1080/07328303.2010.508295