erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine

Base Information

Chemical Name:erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine
CAS No.:135147-79-4
Molecular Formula:C₁₅H₁₈N₂O
Molecular Weight:242.321
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine

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Technology Process of erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine

There total 2 articles about erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 135147-78-3
1-(2-methoxyphenyl)-2-phenylethanedione dioxime

: 135147-79-4
erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine dihydrochloride

Guidance literature:: With sodium tetrahydroborate; titanium tetrachloride; In various solvent(s); for 24h; Ambient temperature;

Reference yield:

: 34082-43-4
2-methoxybenzil

: 135147-79-4
erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine dihydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / H₂NOH*HCl, NaOH / H₂O / 72 h / Ambient temperature

2: 50 percent / NaBH₄, TiCl₄ / various solvent(s) / 24 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; hydroxylamine hydrochloride; titanium tetrachloride; In water;

Reference yield: 71.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 135147-79-4
erythro-1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine

: 135147-86-3
erythro-{1-(2-methoxyphenyl)-2-phenyl-1,2-ethanediamine}diiodoplatinum(II)

Guidance literature:: With potassium iodide; In water; aqueous solution of K2PtCl4 and KI was stirred for 30 min at 50° C; solution was added to an aqueous acidic solution (pH 3,HCl) of the diamine ligand; stirred for 24 h; pH adjusted to 5,5-6,5; precipitate collected; washed with HCl and water; dried with CaCl2/silica gel at 80°C/0,1 Torr; elem. anal.;