bromo(dimesitylsilyl)dimesitylgermane

Base Information

• Chemical Name: bromo(dimesitylsilyl)dimesitylgermane
• CAS No.: 141376-95-6
• Molecular Formula: C₃₆H₄₅BrGeSi
• Molecular Weight: 658.333
• Mol file: 141376-95-6.mol

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Chemical Property of bromo(dimesitylsilyl)dimesitylgermane

Chemical Property:

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Technology Process of bromo(dimesitylsilyl)dimesitylgermane

There total 1 articles about bromo(dimesitylsilyl)dimesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

(chlorodimesitylsilyl)dimesitylgermane (141376-85-4) + benzyl bromide (100-39-0) → bromo(dimesitylsilyl)dimesitylgermane (141376-95-6)

Guidance literature:

With tert.-butyl lithium; In tetrahydrofuran; addn. of t-BuLi in pentanes to a soln. of the silylgermane in THF at -23°C under dry Ar, stirring (6 h, room temp.), addn. of PhCH2Br; aq. workup, washing to crude mixt. with pentanes, chromy.;

DOI:10.1021/om00042a035

upstream raw materials:

(chlorodimesitylsilyl)dimesitylgermane

benzyl bromide