Technology Process of Benzenepropanal, 4-(1,1-diMethylethyl)-2-Methyl-
There total 4 articles about Benzenepropanal, 4-(1,1-diMethylethyl)-2-Methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
for 15h;
Ambient temperature;
DOI:10.1002/hlca.19960790418
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / LiBr, toluene-4-sulfonic acid hydrate / 15 h / Ambient temperature
2: 67 percent / AlCl3 / CH2Cl2 / 1 h / 3 - 4 °C
3: 83 percent / hydrogen / 5percent Pd/C / ethyl acetate; ethanol / 15 h / 760 Torr / Ambient temperature
4: 54 percent / pyridinium chlorochromate / CH2Cl2 / 15 h / Ambient temperature
With
aluminium trichloride; hydrogen; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium bromide;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790418
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / hydrogen / 5percent Pd/C / ethyl acetate; ethanol / 15 h / 760 Torr / Ambient temperature
2: 54 percent / pyridinium chlorochromate / CH2Cl2 / 15 h / Ambient temperature
With
hydrogen; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790418