(CH₃PC₅H(Si(CH₃)3)2(C₆H₅)2)PdCl(P(C₆H₅)3)

Base Information

• Chemical Name: (CH₃PC₅H(Si(CH₃)3)2(C₆H₅)2)PdCl(P(C₆H₅)3)
• CAS No.: 712354-91-1
• Molecular Formula: C₄₂H₄₇ClP₂PdSi₂
• Molecular Weight: 811.827
• Mol file: 712354-91-1.mol

Synonyms:

Chemical Property of (CH₃PC₅H(Si(CH₃)3)2(C₆H₅)2)PdCl(P(C₆H₅)3)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (CH₃PC₅H(Si(CH₃)3)2(C₆H₅)2)PdCl(P(C₆H₅)3)

There total 1 articles about (CH₃PC₅H(Si(CH₃)3)2(C₆H₅)2)PdCl(P(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

bis-triphenylphosphine-palladium(II) chloride (13965-03-2) + 3,5-diphenyl-2,6-bis(trimethylsilyl)phosphinine (184243-21-8) → (CH3PC5H(Si(CH3)3)2(C6H5)2)PdCl(P(C6H5)3) (713116-16-6,712354-91-1)

Guidance literature:

With MeLi; In tetrahydrofuran; diethyl ether; under inert atm. to soln. phosphine in THF at -78°C soln. MeLi inether was added, warmed to room temp., cooled to -78°C, (PdCl2(P Ph3)2) was added and stirred at this temp. for 6 h, soln. was allowed towarm to room temp. over 14 h; react. mixt. was extd. with CH2Cl2, solvent was removed, residue was washed with ether; elem. anal.;

DOI:10.1021/om049871y

upstream raw materials:

bis-triphenylphosphine-palladium(II) chloride

3,5-diphenyl-2,6-bis(trimethylsilyl)phosphinine