C₂₀H₂₇N₃O₅S

Base Information

Chemical Name:C₂₀H₂₇N₃O₅S
CAS No.:1428768-75-5
Molecular Formula:C₂₀H₂₇N₃O₅S
Molecular Weight:421.517
Hs Code.:

C<sub>20</sub>H<sub>27</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₇N₃O₅S

Chemical Property:

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Technology Process of C₂₀H₂₇N₃O₅S

There total 9 articles about C₂₀H₂₇N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428768-71-1
C₁₉H₂₅N₃O₃

: 124-63-0
methanesulfonyl chloride

: 1428768-75-5
C₂₀H₂₇N₃O₅S

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2013.02.009

Reference yield:

: 1270290-36-2,1198185-81-7
(R)-2-amino-2-cyclopropylethan-1-ol

: 1428768-75-5
C₂₀H₂₇N₃O₅S

Guidance literature:: Multi-step reaction with 9 steps

1: potassium carbonate / dichloromethane; water / 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 20 °C

3: trifluoroacetic acid / 20 °C

4: potassium iodide; potassium carbonate / acetonitrile / 18 h / 55 °C

5: toluene / 15.25 h / -78 - 55 °C

6: sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / 20 °C

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 18 h / 175 °C

8: boron tribromide / dichloromethane / -78 °C

9: triethylamine / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hexamethyldisilazane; boron tribromide; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2013.02.009

Reference yield:

: 1428768-69-7
C₂₅H₂₈BrN₃O₃

: 1428768-75-5
C₂₀H₂₇N₃O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 18 h / 175 °C

2: boron tribromide / dichloromethane / -78 °C

3: triethylamine / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.02.009