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Technology Process of Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2

Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2

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  • Chemical Name:Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2
  • CAS No.:280573-59-3
  • Molecular Formula:C22H29N5O11S*Gd*Na
  • Molecular Weight:751.805
  • Hs Code.:
Gd<sup>(3+)</sup>*Na<sup>(1+)</sup>*(COOCH<sub>2</sub>NCH<sub>2</sub>COO)2(CH<sub>2</sub>)7NCONHC<sub>6</sub>H<sub>4</sub>SO<sub>2</sub>NH<sub>2</sub><sup>(4-)</sup>=GdNa(COOCH<sub>2</sub>NCH<sub>2</sub> COO)2(CH<sub>2</sub>)7NCONHC<sub>6</sub>H<sub>4</sub>SO<sub>2</sub>NH<sub>2</sub>

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Chemical Property of Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2
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Technology Process of Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2

There total 1 articles about Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

gadolinium(III) chloride hexahydrate

gadolinium(III) chloride hexahydrate

sodium hydroxide
1310-73-2

sodium hydroxide

{[2-([2-(bis-carboxymethyl-amino)-ethyl]-{[2-(4-sulfamoyl-phenyl)-ethylcarbamoyl]-methyl}-amino)-ethyl]-carboxymethyl-amino}-acetic acid
280563-35-1

{[2-([2-(bis-carboxymethyl-amino)-ethyl]-{[2-(4-sulfamoyl-phenyl)-ethylcarbamoyl]-methyl}-amino)-ethyl]-carboxymethyl-amino}-acetic acid

Gd<sup>(3+)</sup>*Na<sup>(1+)</sup>*(COOCH<sub>2</sub>NCH<sub>2</sub>COO)2(CH<sub>2</sub>)7NCONHC<sub>6</sub>H<sub>4</sub>SO<sub>2</sub>NH<sub>2</sub><sup>(4-)</sup>=GdNa(COOCH<sub>2</sub>NCH<sub>2</sub> COO)2(CH<sub>2</sub>)7NCONHC<sub>6</sub>H<sub>4</sub>SO<sub>2</sub>NH<sub>2</sub>
280573-59-3

Gd(3+)*Na(1+)*(COOCH2NCH2COO)2(CH2)7NCONHC6H4SO2NH2(4-)=GdNa(COOCH2NCH2 COO)2(CH2)7NCONHC6H4SO2NH2

Guidance literature:
In water; ligand was dissolved in H2O, aq. soln. of NaOH was added, at pH 7 aq. soln. of GdCl3*6H2O was added slowly, aq. soln. of NaOH was added; dissolved in H2O, loaded onto Amberlite XAD 1600 resin column, eluted with CH3CN/H2O, evapd.;
DOI:10.1002/(sici)1099-0682(200004)2000:4<625::aid-ejic625>3.0.co;2-2
upstream raw materials:

sodium hydroxide

{[2-([2-(bis-carboxymethyl-amino)-ethyl]-{[2-(4-sulfamoyl-phenyl)-ethylcarbamoyl]-methyl}-amino)-ethyl]-carboxymethyl-amino}-acetic acid

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