2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester
CAS No.:316808-34-1
Molecular Formula:C₂₇H₄₆O₁₀
Molecular Weight:530.656
Hs Code.:

Synonyms:

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Chemical Property of 2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

Chemical Property:

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Technology Process of 2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

There total 15 articles about 2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68426-09-5
(4-methoxyphenoxy)acetaldehyde

: 316808-34-1
2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 91 percent / diethyl ether / -78 °C

2: 96 percent / iPr₂NEt / CH₂Cl₂ / 25 °C

3: 90 percent / 9-BBN; NaOH; H₂O₂ / tetrahydrofuran

4: 88 percent / PCC / CH₂Cl₂ / 25 °C

5: 92 percent / diethyl ether / 4 h / -78 °C

6: 0.112 g / OsO₄; NMO; NaIO₄ / acetone; H₂O; 2-methyl-propan-2-ol / 0.5 h / 25 °C

7: 92 percent / diethyl ether / 4 h / -78 °C

8: 90 percent / iPr₂NEt / CH₂Cl₂ / 25 °C

9: OsO₄; NMO; NaIO₄ / acetone; H₂O / 25 °C

10: NaBH₄ / methanol / 0 °C

11: pyridine / 25 °C

With sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; 9-borabicyclo[3.3.1]nonane dimer; N-methyl-2-indolinone; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; water; acetone; tert-butyl alcohol; 1: Alkylation / 2: Alkylation / 3: Oxidation / 4: Oxidation / 5: Alkylation / 6: Oxidation / 7: Alkylation / 8: Alkylation / 9: Oxidation / 10: Reduction / 11: Acylation;
DOI:10.1021/ol0063914

Reference yield:

: 2211-94-1,51469-79-5,71048-65-2,71031-04-4,26744-15-0
4-methoxybenzyloxy ester of (S)-glycidol

: 316808-34-1
2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: tetrahydrofuran / 0 °C

2: iPr₂NEt / CH₂Cl₂ / 25 °C

3: 90 percent / OsO₄; NMO; NaIO₄ / acetone; H₂O

4: 92 percent / diethyl ether / 4 h / -78 °C

5: 0.112 g / OsO₄; NMO; NaIO₄ / acetone; H₂O; 2-methyl-propan-2-ol / 0.5 h / 25 °C

6: 92 percent / diethyl ether / 4 h / -78 °C

7: 90 percent / iPr₂NEt / CH₂Cl₂ / 25 °C

8: OsO₄; NMO; NaIO₄ / acetone; H₂O / 25 °C

9: NaBH₄ / methanol / 0 °C

10: pyridine / 25 °C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; pyridine; methanol; diethyl ether; dichloromethane; water; acetone; tert-butyl alcohol; 1: Grignard reaction / 2: Alkylation / 3: Oxidation / 4: Alkylation / 5: Oxidation / 6: Alkylation / 7: Alkylation / 8: Oxidation / 9: Reduction / 10: Acylation;
DOI:10.1021/ol0063914

Reference yield:

: 150-76-5
4-methoxy-phenol

: 316808-34-1
2,2-Dimethyl-propionic acid (3S,5R,8R)-3,5,8-tris-methoxymethoxy-9-(4-methoxy-phenoxy)-nonyl ester

Guidance literature:: Multi-step reaction with 11 steps

1: 80 percent / PPH₃; DEAD / ethanol / 25 °C

2: tetrahydrofuran / 0 °C

3: iPr₂NEt / CH₂Cl₂ / 25 °C

4: 90 percent / OsO₄; NMO; NaIO₄ / acetone; H₂O

5: 92 percent / diethyl ether / 4 h / -78 °C

6: 0.112 g / OsO₄; NMO; NaIO₄ / acetone; H₂O; 2-methyl-propan-2-ol / 0.5 h / 25 °C

7: 92 percent / diethyl ether / 4 h / -78 °C

8: 90 percent / iPr₂NEt / CH₂Cl₂ / 25 °C

9: OsO₄; NMO; NaIO₄ / acetone; H₂O / 25 °C

10: NaBH₄ / methanol / 0 °C

11: pyridine / 25 °C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; dichloromethane; water; acetone; tert-butyl alcohol; 1: Alkylation / 2: Grignard reaction / 3: Alkylation / 4: Oxidation / 5: Alkylation / 6: Oxidation / 7: Alkylation / 8: Alkylation / 9: Oxidation / 10: Reduction / 11: Acylation;
DOI:10.1021/ol0063914