Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)

Base Information

Chemical Name:Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)
CAS No.:238432-90-1
Molecular Formula:C₅₄H₄₈P₂Ru
Molecular Weight:859.993
Hs Code.:

Ru(C<sub>9</sub>H<sub>7</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2(CCCHC(CH<sub>2</sub>)5)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)

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Technology Process of Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)

There total 1 articles about Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 182746-98-1
[Ru(-C*C-CH2PPh3)(η(5-)-indenyl)(PPh3)2](hexafluorophosphate)

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 238432-90-1
Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; (N2); addn. of n-BuLi in hexane to Ru complex in THF at -20°C, stirring 15 min, addn. of the org. carbonyl compd., warming to room temp.,further stirring (15 min); solvent removal (vac.), chromy. (Alox I; hexane/Et2O 1:1); elem. anal.;

Reference yield: 70.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 238432-90-1
Ru(C₉H₇)(P(C₆H₅)3)2(CCCHC(CH₂)5)

: Ru(C₉H₇)(P(C₆H₅)3)2(CCHCHC(CH₂)5)⁽¹⁺⁾*BF₄^(1-) = [Ru(C₉H₇)(P(C₆H₅)3)2(CCHCHC(CH₂)5)]BF₄

Guidance literature:: In tetrahydrofuran; diethyl ether; (N2); dropwise addn. of HBF4*OEt2 in Et2O at -20°C to Ru complex in THF, gradual warming to room temp.; concn., pptn. by addn. of Et2O, collection, washing (Et2O), drying (vac.); elem. anal.;