hypercloso-B₄(CH₂(t)Bu)4

Base Information

• Chemical Name: hypercloso-B₄(CH₂(t)Bu)4
• CAS No.: 237741-11-6
• Molecular Formula: C₂₀H₄₄B₄
• Molecular Weight: 327.813
• Mol file: 237741-11-6.mol

Synonyms:

Chemical Property of hypercloso-B₄(CH₂(t)Bu)4

Chemical Property:

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Safty Information:

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Useful:

Technology Process of hypercloso-B₄(CH₂(t)Bu)4

There total 1 articles about hypercloso-B₄(CH₂(t)Bu)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.2%

(CH3)3CCH2BF2 (237741-23-0) → hypercloso-B4(CH2(t)Bu)4 (237741-11-6) + potassium neopentyltrifluoroborate (1150655-02-9)

Guidance literature:

With Na/K alloy; In pentane; stirring for 2 h (spontaneous boling); filtration, washing of residue (pentane), evapn. of filtrates (vac.,), distn. (90°C, 0.001 mbar); K-salt from residue after filtration onextn. with THF;

DOI:10.1016/s0020-1693(99)00058-4

upstream raw materials:

(CH₃)3CCH₂BF₂