1-{[(4-chlorophenyl)imino]methyl}-2-naphthol

Base Information

• Chemical Name: 1-{[(4-chlorophenyl)imino]methyl}-2-naphthol
• CAS No.: 894-95-1
• Molecular Formula: C17H12ClNO
• Molecular Weight: 281.741

Synonyms:2-hydroxy-1-naphthalidene-4'-chloro-anil;2-Hydroxy-1-naphthalidene-4'-chloroaniline;2-hydroxy-1-naphthalideneaniline-4-Cl;N-2-hydroxy-1-naphthaldimine-p-chloroaniline;

Chemical Property of 1-{[(4-chlorophenyl)imino]methyl}-2-naphthol

Chemical Property:

• PSA: 32.59000
• LogP: 4.94940

Purity/Quality:

99% ^*data from raw suppliers

1-(4-CHLOROPHENYLIMINOMETHYL)-2-NAPHTHOL Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-{[(4-chlorophenyl)imino]methyl}-2-naphthol

There total 3 articles about 1-{[(4-chlorophenyl)imino]methyl}-2-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-chloro-aniline (106-47-8) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 1-((4-chlorophenylimino)methyl)naphthalen-2-ol (894-95-1)

Guidance literature:

With aqueous extract of pericarp of Sapindus trifoliatus fruits; at 20 ℃; for 0.0333333h;

DOI:10.1002/cbdv.200900272

Reference yield:

4-chlorobenzonitrile (100-00-5) → 1-((4-chlorophenylimino)methyl)naphthalen-2-ol (894-95-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate; chloro(p-cymene)(1-((4-nitrophenylimino)methyl)naphthalen-2-ol-κ-O,N)ruthenium(II) / ethanol / 2 h / 20 °C / Inert atmosphere; Schlenk technique

2: acetic acid / methanol / 3 h / 75 °C / Inert atmosphere; Schlenk technique

With sodium tetrahydroborate; chloro(p-cymene)(1-((4-nitrophenylimino)methyl)naphthalen-2-ol-κ-O,N)ruthenium(II); acetic acid; In methanol; ethanol;

DOI:10.1080/00958972.2017.1284322

Reference yield:

→ 1-((4-chlorophenylimino)methyl)naphthalen-2-ol (894-95-1)

Guidance literature:

2-Hydroxy-1-naphthylaldehyd, p-Chloranilin;

upstream raw materials:

4-chloro-aniline

2-hydroxynaphthalene-1-carbaldehyde

4-chlorobenzonitrile

Downstream raw materials:

(4-Chloro-phenyl)-(1,2-dihydro-naphtho[2,1-b]furan-1-yl)-amine

VO(2-hydroxyl-1-naphthalidene-4'-chloroanil)2

C₆H₅AsO₃^(2-)*Al⁽³⁺⁾*ClC₆H₄NCHC₁₀H₆O^(1-) = C₆H₅AsO₃Al(OC₁₀H₆CHNC₆H₄Cl)

RuBr₂(AsPh₃)2(NCA)

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