[(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

Base Information

Chemical Name:[(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate
CAS No.:1235259-83-2
Molecular Formula:C₇H₈*C₅₄H₅₂Ge₃
Molecular Weight:1010.92
Hs Code.:

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Chemical Property of [(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

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Technology Process of [(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

There total 3 articles about [(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1235259-89-8
[(p-tolyl)3(germanium)(NMe₂)]

: 1675-58-7
diphenylgermane

: 108-88-3,15644-74-3,16713-13-6
toluene

: 75-05-8,26809-02-9
acetonitrile

: 1235259-83-2
[(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

Guidance literature:: In acetonitrile; byproducts: HNMe2; Schlenk technique, under N2; to Ph2GeH2 (0.437 mmol) soln. added Tol3GeNMe2 (0.874 mmol) soln., stirred for 48 h at 90°C, volatiles removed in vac., distilled, recrystd. from hot toluene; elem. anal.;
DOI:10.1016/j.jorganchem.2010.04.015

Reference yield:

: 106-43-4
para-chlorotoluene

: 1235259-83-2
[(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HCl; Mg; I₂ / tetrahydrofuran

2: benzene

3: acetonitrile

With aq. HCl; Mg; I₂; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1016/j.jorganchem.2010.04.015

Reference yield:

: 58436-48-9
tri(p-tolyl)chlorogermane

: 1235259-83-2
[(p-tolyl)3(germanium)2(phenyl)2(germanium)(p-tolyl)3] toluene monosolvate

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: acetonitrile

In acetonitrile; benzene;
DOI:10.1016/j.jorganchem.2010.04.015