WBr₂(CO)3(CH₃C₆H₄N⁽¹⁵⁾NNP(C₆H₅)3)

Base Information

• Chemical Name: WBr₂(CO)3(CH₃C₆H₄N⁽¹⁵⁾NNP(C₆H₅)3)
• CAS No.: 80594-74-7
• Molecular Formula: C₂₈H₂₂Br₂N₃O₃PW
• Molecular Weight: 824.126
• Mol file: 80594-74-7.mol

Synonyms:

Chemical Property of WBr₂(CO)3(CH₃C₆H₄N⁽¹⁵⁾NNP(C₆H₅)3)

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of WBr₂(CO)3(CH₃C₆H₄N⁽¹⁵⁾NNP(C₆H₅)3)

There total 1 articles about WBr₂(CO)3(CH₃C₆H₄N⁽¹⁵⁾NNP(C₆H₅)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

WBr2(CO)3(P(C6H5)3)2 (18130-07-9,135820-70-1) + (15)NN2(C6H4CH3) (2101-86-2) → WBr2(CO)3(CH3C6H4N(15)NNP(C6H5)3) (80594-74-7)

Guidance literature:

In dichloromethane; W complex in CH2Cl2 addding to a labeled ligand soln. in cyclopentane under N2, stirring for 10 min at 20°C, filtering, solvent removingin vacuo, Et2O adding dropwise, ppt. collecting, washing with warm abs.EtOH; identified by IR and NMR spectra;

DOI:10.1021/ic00135a068

upstream raw materials:

WBr₂(CO)3(P(C₆H₅)3)2

⁽¹⁵⁾NN₂(C₆H₄CH₃)