[2,6-bis((diethylamino)methyl)phenyl]GeOC₆H₂-2,4,6-Me₃

Base Information

• Chemical Name: [2,6-bis((diethylamino)methyl)phenyl]GeOC₆H₂-2,4,6-Me₃
• CAS No.: 444718-13-2
• Molecular Formula: C₂₅H₃₈GeN₂O
• Molecular Weight: 455.18
• Mol file: 444718-13-2.mol

Synonyms:

Chemical Property of [2,6-bis((diethylamino)methyl)phenyl]GeOC₆H₂-2,4,6-Me₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2,6-bis((diethylamino)methyl)phenyl]GeOC₆H₂-2,4,6-Me₃

There total 2 articles about [2,6-bis((diethylamino)methyl)phenyl]GeOC₆H₂-2,4,6-Me₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[2,6-bis((diethylamino)methyl)phenyl]GeN((i)Pr)2 + Mesitol (527-60-6) → [2,6-bis((diethylamino)methyl)phenyl]GeOC6H2-2,4,6-Me3 (444718-13-2)

Guidance literature:

In tetrahydrofuran; under N2 atm. soln. MesOH in THF was added slowly to soln. ArGeN(i-Pr)2 in THF at -78°C, stirred for 30 min and heated at reflux for 1 h; solvent was removed under vac.; elem. anal.;

DOI:10.1021/om020187y

Reference yield:

chloro[2,6-bis[(diethylamino)methyl]phenyl]germylene (444718-17-6) → [2,6-bis((diethylamino)methyl)phenyl]GeOC6H2-2,4,6-Me3 (444718-13-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether

2: tetrahydrofuran

In tetrahydrofuran; diethyl ether;

DOI:10.1021/om020187y

upstream raw materials:

Mesitol

chloro[2,6-bis[(diethylamino)methyl]phenyl]germylene