4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]

Base Information

Chemical Name:4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]
CAS No.:87367-66-6
Molecular Formula:C₁₈H₁₈O₄
Molecular Weight:298.339
Hs Code.:
DSSTox Substance ID:DTXSID601194024

Synonyms:DTXSID601194024;AKOS005367832;87367-66-6;4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]

Suppliers and Price of 4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:298.12050905
Heavy Atom Count:22
Complexity:328

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(CCOC1=CC=C(C=C1)C=O)OC2=CC=C(C=C2)C=O

Technology Process of 4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde]

There total 1 articles about 4,4'-[(1-Methyl-1,3-propanediyl)bis(oxy)]bis[benzaldehyde] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 87367-66-6
C₁₈H₁₈O₄

Guidance literature:: With sodium ethanolate; Yield given. Multistep reaction; 1.) ethanol, reflux, 4 h, 2.) reflux, 48 h;
DOI:10.1007/BF00765771

Reference yield: 84.5%

: 87367-66-6
C₁₈H₁₈O₄

: 105-53-3
diethyl malonate

: 87367-70-2
2-(4-{3-[4-(2,2-Bis-ethoxycarbonyl-vinyl)-phenoxy]-1-methyl-propoxy}-benzylidene)-malonic acid diethyl ester

Guidance literature:: With piperidine; acetic acid; In benzene; Heating;
DOI:10.1007/BF00765771

Reference yield:

: 87367-66-6
C₁₈H₁₈O₄

: 87367-90-6
C₂₄H₂₄N₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1: 84.5 percent / piperidine, glacial acetic acid / benzene / Heating

2: 2.) NaOH / 1.) water, ethanol, heating, 2 h, 2.) ethylene glycol, heating, 40 h

3: 1.) acetic anhydride, 2.) ammonia / 1.) heating, 6 h, 2.) ethyl acetate, 2 h

4: 1 h / 200 - 220 °C

With piperidine; sodium hydroxide; ammonia; acetic anhydride; acetic acid; In benzene;
DOI:10.1007/BF00765771