2-METHYLFURO[3,2-C]PYRIDIN-4-OL

Base Information

Chemical Name:2-METHYLFURO[3,2-C]PYRIDIN-4-OL
CAS No.:26956-44-5
Molecular Formula:C8H7NO2
Molecular Weight:149.149
Hs Code.:2934999090
Mol file:26956-44-5.mol

Synonyms:2-Methyl-4-oxo-4,5-dihydrofuro<3,2-c>pyridin;;2-METHYLFURO[3,2-C]PYRIDIN-4-OL;;2-methylfuro[3,2-c]pyridin-4(5H)-one;;4,5-Dihydro-2-methyl-4-oxo-furo<3,2-c>pyridine;;

Suppliers and Price of 2-METHYLFURO[3,2-C]PYRIDIN-4-OL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
2-Methylfuro[3,2-c]pyridin-4(5H)-one
10g
$ 3141.00

Total 8 raw suppliers

Chemical Property of 2-METHYLFURO[3,2-C]PYRIDIN-4-OL

Chemical Property:

Boiling Point:382.7±42.0°C at 760 mmHg (Cal.) ref.
PKA:12.77±0.20(Predicted)
Flash Point:185.2±27.9°C (Cal.) ref.
PSA：46.00000
Density:1.2±0.1g/cm3 (Cal.) ref.
LogP:1.42950

Purity/Quality:

98%min ^*data from raw suppliers

2-Methylfuro[3,2-c]pyridin-4(5H)-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-METHYLFURO[3,2-C]PYRIDIN-4-OL

There total 7 articles about 2-METHYLFURO[3,2-C]PYRIDIN-4-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 220992-24-5
2-methylfuro<3,2-c>pyridine N-oxide

: 26956-44-5
2-methylfuro<3,2-c>pyridin-4(5H)-one

Guidance literature:: With acetic anhydride; for 1.5h; Heating;
DOI:10.1002/jhet.5570350601

Reference yield:

: 14779-25-0
3-(5-methylfuran-2-yl) acrylic acid

: 26956-44-5
2-methylfuro<3,2-c>pyridin-4(5H)-one

Guidance literature:: Multistep reaction; (i) ClCO₂Et, Et₃N, acetone, (ii) aq. NaNO₂, (iii) nBu₃N, Ph₂CH₂;

Reference yield:

: 31270-83-4
2-methylfuro<3,2-c>pyridine

: 26956-44-5
2-methylfuro<3,2-c>pyridin-4(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / m-CPBA / CHCl₃ / 15 h / Ambient temperature

2: 52 percent / Ac₂O / 1.5 h / Heating

With acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1002/jhet.5570350601