C₁₇H₂₃NO₄

Base Information

• Chemical Name: C₁₇H₂₃NO₄
• CAS No.: 1402155-07-0
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Mol file: 1402155-07-0.mol

Synonyms:

Chemical Property of C₁₇H₂₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₄

There total 6 articles about C₁₇H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-O-(1-methylethylidene)-α-D-lyxo-pentodialdo-1,4-furanose + acetic anhydride (108-24-7) + sodium cyanoborohydride (25895-60-7) + benzylamine (100-46-9) → C17H23NO4 (1402155-07-0) + C18H22N2O4 (1402155-08-1)

Guidance literature:

2,3-O-(1-methylethylidene)-α-D-lyxo-pentodialdo-1,4-furanose; sodium cyanoborohydride; benzylamine; In methanol; at 20 ℃; for 120h;

acetic anhydride; With pyridine; In methanol; at 20 ℃;

DOI:10.1002/ejoc.201200587

Reference yield:

D-Mannose (530-26-7) → C17H23NO4 (1402155-07-0)

Guidance literature:

Multi-step reaction with 6 steps

1.1: iodine / 2 h / 20 °C

2.1: 18-crown-6 ether; potassium hydroxide / tetrahydrofuran / 16 h / 20 °C

3.1: acetic acid / water / 18 h / 20 °C

4.1: silica-gel supported NaIO₄ / dichloromethane / 0.83 h / 20 °C

5.1: 20 % Pd(OH)2/C; hydrogen / methanol / 4 h / 20 °C

6.1: methanol / 120 h / 20 °C

6.2: 20 °C

With 18-crown-6 ether; 20 % Pd(OH)2/C; hydrogen; iodine; acetic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1002/ejoc.201200587

Reference yield:

2,3,5,6-di-O-isopropylidene-D-mannofuranose (7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4) → C17H23NO4 (1402155-07-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 18-crown-6 ether; potassium hydroxide / tetrahydrofuran / 16 h / 20 °C

2.1: acetic acid / water / 18 h / 20 °C

3.1: silica-gel supported NaIO₄ / dichloromethane / 0.83 h / 20 °C

4.1: 20 % Pd(OH)2/C; hydrogen / methanol / 4 h / 20 °C

5.1: methanol / 120 h / 20 °C

5.2: 20 °C

With 18-crown-6 ether; 20 % Pd(OH)2/C; hydrogen; acetic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1002/ejoc.201200587

upstream raw materials:

acetic anhydride

sodium cyanoborohydride

benzylamine

2,3,5,6-di-O-isopropylidene-D-mannofuranose