5'-O-acetyl-3'-O-<carbamoyl>thymidine

Base Information

Chemical Name:5'-O-acetyl-3'-O-<carbamoyl>thymidine
CAS No.:129835-23-0
Molecular Formula:C₂₁H₃₂N₅O₈P
Molecular Weight:513.488
Hs Code.:

5'-O-acetyl-3'-O-<<bis(2,2-dimethyl-1-aziridinyl)phosphinyl>carbamoyl>thymidine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-acetyl-3'-O-<carbamoyl>thymidine

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Technology Process of 5'-O-acetyl-3'-O-<carbamoyl>thymidine

There total 6 articles about 5'-O-acetyl-3'-O-<carbamoyl>thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2658-24-4
2,2-dimethylaziridine

: C₁₃H₁₆Cl₂N₃O₈P

: 129835-23-0
5'-O-acetyl-3'-O-<carbamoyl>thymidine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 5 ℃; for 17h; Yield given;
DOI:10.1021/jm00171a039

Reference yield:

: 35898-31-8
5'-O-acetylthymidine

: 129835-23-0
5'-O-acetyl-3'-O-<carbamoyl>thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 0 - 5 °C

2: Et₃N / tetrahydrofuran / 17 h / 0 - 5 °C

With triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00171a039

Reference yield:

: Acetic acid (2R,3S,5R)-3-[(4-methoxy-phenyl)-diphenyl-methoxy]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

: 129835-23-0
5'-O-acetyl-3'-O-<carbamoyl>thymidine

Guidance literature:: Multi-step reaction with 3 steps

1: 80percent acetic acid / 1.5 h / Ambient temperature

2: tetrahydrofuran / 1 h / 0 - 5 °C

3: Et₃N / tetrahydrofuran / 17 h / 0 - 5 °C

With acetic acid; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00171a039