C₂₅H₃₄O₅

Base Information

Chemical Name:C₂₅H₃₄O₅
CAS No.:93097-31-5
Molecular Formula:C₂₅H₃₄O₅
Molecular Weight:414.542
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₄O₅

Chemical Property:

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Technology Process of C₂₅H₃₄O₅

There total 9 articles about C₂₅H₃₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4695-62-9,126-21-6
fenchone

: 93097-31-5
C₂₅H₃₄O₅

Guidance literature:: Multi-step reaction with 9 steps

2: 84 percent / m-chloroperbenzoic acid, disodium hydrogen phosphate / CH₂Cl₂ / at 0 grad C for 6 h then at R_.t. for 18 h

3: 2.) chromium trioxide-pyridine / 1.) methanol, 30 grad C, 2 h 2.) CH₂Cl₂

5: 40 percent / LDA / tetrahydrofuran / 2 h / 0 °C

6: 79 percent / HCl / H₂O; methanol / 3 h / 25 °C

7: 77 percent / potassium t-butoxide / benzene; 2-methyl-propan-2-ol / 0.25 h

With hydrogenchloride; disodium hydrogenphosphate; chromium trioxide pyridine; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; benzene;
DOI:10.1016/0040-4039(84)80119-7

Reference yield:

: 93220-60-1
Β-Fenchocamphorone

: 93097-31-5
C₂₅H₃₄O₅

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / m-chloroperbenzoic acid, disodium hydrogen phosphate / CH₂Cl₂ / at 0 grad C for 6 h then at R_.t. for 18 h

2: 2.) chromium trioxide-pyridine / 1.) methanol, 30 grad C, 2 h 2.) CH₂Cl₂

4: 40 percent / LDA / tetrahydrofuran / 2 h / 0 °C

5: 79 percent / HCl / H₂O; methanol / 3 h / 25 °C

6: 77 percent / potassium t-butoxide / benzene; 2-methyl-propan-2-ol / 0.25 h

With hydrogenchloride; disodium hydrogenphosphate; chromium trioxide pyridine; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; benzene;
DOI:10.1016/0040-4039(84)80119-7

Reference yield:

: 93097-25-7
(1R,5R)-6,6-Dimethyl-2-oxa-bicyclo[3.2.1]octan-3-one

: 93097-31-5
C₂₅H₃₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: 2.) chromium trioxide-pyridine / 1.) methanol, 30 grad C, 2 h 2.) CH₂Cl₂

3: 40 percent / LDA / tetrahydrofuran / 2 h / 0 °C

4: 79 percent / HCl / H₂O; methanol / 3 h / 25 °C

5: 77 percent / potassium t-butoxide / benzene; 2-methyl-propan-2-ol / 0.25 h

With hydrogenchloride; chromium trioxide pyridine; potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; methanol; water; tert-butyl alcohol; benzene;
DOI:10.1016/0040-4039(84)80119-7