C₁₅H₁₈O₅

Base Information

Chemical Name:C₁₅H₁₈O₅
CAS No.:1311379-26-6
Molecular Formula:C₁₅H₁₈O₅
Molecular Weight:278.305
Hs Code.:

C<sub>15</sub>H<sub>18</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₈O₅

Chemical Property:

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Technology Process of C₁₅H₁₈O₅

There total 6 articles about C₁₅H₁₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311379-42-6
C₁₆H₃₀O₄Si

: 1311379-26-6
C₁₅H₁₈O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

1.2: 0 - 45 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / Inert atmosphere

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C

4.1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

5.1: sulfuric acid / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium phosphate monobasic monohydrate; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 2-methyl-but-2-ene; water; ethyl acetate; mineral oil; tert-butyl alcohol; 4.1: Pinnick oxidation;
DOI:10.1021/ja203642n

Reference yield:

: C₁₇H₂₀O₄

: 1311379-26-6
C₁₅H₁₈O₅

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

2: sulfuric acid / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium phosphate monobasic monohydrate; sulfuric acid; In 2-methyl-but-2-ene; water; tert-butyl alcohol; 1: Pinnick oxidation;
DOI:10.1021/ja203642n

Reference yield:

: 1311379-25-5
C₁₇H₂₂O₄

: 1311379-26-6
C₁₅H₁₈O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C

2: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C

3: sulfuric acid / 0 - 20 °C / Inert atmosphere

With sodium chlorite; sodium phosphate monobasic monohydrate; sulfuric acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In 2-methyl-but-2-ene; water; ethyl acetate; tert-butyl alcohol; 2: Pinnick oxidation;
DOI:10.1021/ja203642n