C₄₂H₅₆N₄O₂₄

Base Information

Chemical Name:C₄₂H₅₆N₄O₂₄
CAS No.:1176981-37-5
Molecular Formula:C₄₂H₅₆N₄O₂₄
Molecular Weight:1000.92
Hs Code.:

C<sub>42</sub>H<sub>56</sub>N<sub>4</sub>O<sub>24</sub>

Synonyms:

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Chemical Property of C₄₂H₅₆N₄O₂₄

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Technology Process of C₄₂H₅₆N₄O₂₄

There total 10 articles about C₄₂H₅₆N₄O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 1176981-37-5
C₄₂H₅₆N₄O₂₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

1.2: Dowex H+

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

3.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

4.1: water; acetic acid / dichloromethane / 48 h / 20 °C

5.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

5.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

6.1: sodium methylate / methanol / 0.33 h / 20 °C

6.2: Dowex H+

7.1: hydrazine / ethanol / 70 °C

8.1: dmap / pyridine / 2 h / 20 °C

9.1: pyridine / 20 °C

With dmap; N-iodo-succinimide; water; sodium methylate; toluene-4-sulfonic acid; acetic acid; hydrazine; In pyridine; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1316823-20-7
p-nitrophenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

: 1176981-37-5
C₄₂H₅₆N₄O₂₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; acetic acid / dichloromethane / 48 h / 20 °C

2.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

3.1: sodium methylate / methanol / 0.33 h / 20 °C

3.2: Dowex H+

4.1: hydrazine / ethanol / 70 °C

5.1: dmap / pyridine / 2 h / 20 °C

6.1: pyridine / 20 °C

With dmap; N-iodo-succinimide; water; sodium methylate; acetic acid; hydrazine; In pyridine; methanol; ethanol; dichloromethane;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1316823-24-1
p-nitrophenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-(1->3)-2-azido-2-deoxy-α-D-galactopyranoside

: 1176981-37-5
C₄₂H₅₆N₄O₂₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 0.33 h / 20 °C

2.2: Dowex H+

3.1: hydrazine / ethanol / 70 °C

4.1: dmap / pyridine / 2 h / 20 °C

5.1: pyridine / 20 °C

With dmap; N-iodo-succinimide; sodium methylate; hydrazine; In pyridine; methanol; ethanol; dichloromethane;
DOI:10.1016/j.carres.2011.03.036