(2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

Base Information

Chemical Name:(2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol
CAS No.:178150-84-0
Molecular Formula:C₂₂H₄₄O₄
Molecular Weight:372.589
Hs Code.:

Synonyms:

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Chemical Property of (2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

Chemical Property:

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Technology Process of (2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

There total 7 articles about (2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765-09-3
1-bromotridecane

: 178150-84-0
(2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / acetonitrile / 24 h / Heating

2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, from 0 deg C to RT, 1 h

3: 95 percent / H₂ / 10percent Pd/C / methanol / 0.33 h / 103.4 Torr

4: 75 percent / pyridine / 18 h / Ambient temperature

5: 95 percent / KOH / benzene / 1 h

6: 1.) NaH / 1.) DMSO, RT, 1 h, 2.) DMSO, RT, 5 d

With pyridine; potassium hydroxide; n-butyllithium; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; acetonitrile; benzene;
DOI:10.1016/0040-4020(96)00278-5

Reference yield:

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

: 178150-84-0
(2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, from 0 deg C to RT, 1 h

2: 95 percent / H₂ / 10percent Pd/C / methanol / 0.33 h / 103.4 Torr

3: 75 percent / pyridine / 18 h / Ambient temperature

4: 95 percent / KOH / benzene / 1 h

5: 1.) NaH / 1.) DMSO, RT, 1 h, 2.) DMSO, RT, 5 d

With pyridine; potassium hydroxide; n-butyllithium; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; benzene;
DOI:10.1016/0040-4020(96)00278-5

Reference yield:

: 544-63-8
n-tetradecanoic acid

: 178150-84-0
(2S,2'S)-1'-O-(2'-hydroxyhexadecyl)-2,3-O-isopropylidene glycerol

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / Br₂, HgO red / CCl₄ / 1.5 h / Heating

2: 90 percent / acetonitrile / 24 h / Heating

3: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) THF, hexane, from 0 deg C to RT, 1 h

4: 95 percent / H₂ / 10percent Pd/C / methanol / 0.33 h / 103.4 Torr

5: 75 percent / pyridine / 18 h / Ambient temperature

6: 95 percent / KOH / benzene / 1 h

7: 1.) NaH / 1.) DMSO, RT, 1 h, 2.) DMSO, RT, 5 d

With pyridine; potassium hydroxide; n-butyllithium; hydrogen; bromine; sodium hydride; mercury(II) oxide; palladium on activated charcoal; In methanol; tetrachloromethane; acetonitrile; benzene;
DOI:10.1016/0040-4020(96)00278-5