Triphenyltridecylphosphonium Bromide

Base Information

Chemical Name:Triphenyltridecylphosphonium Bromide
CAS No.:13266-02-9
Molecular Formula:C31H42P.Br
Molecular Weight:525.552
Hs Code.:2931900090
Mol file:13266-02-9.mol

Synonyms:Triphenyltridecylphosphonium Bromide;

Suppliers and Price of Triphenyltridecylphosphonium Bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
TriphenyltridecylphosphoniumBromide
250mg
$ 155.00

Total 4 raw suppliers

Chemical Property of Triphenyltridecylphosphonium Bromide

Chemical Property:

Melting Point:84-86°C
PSA：13.59000
LogP:5.29550
Storage Temp.:Refrigerator
Solubility.:Dichloromethane, Methanol

Purity/Quality:

97% ^*data from raw suppliers

TriphenyltridecylphosphoniumBromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Wittig Reagents.

Technology Process of Triphenyltridecylphosphonium Bromide

There total 7 articles about Triphenyltridecylphosphonium Bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 116754-58-6
13-bromo-1-tridecylalcohol

: 603-35-0
triphenylphosphine

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

Guidance literature:: In acetonitrile; for 48h; Solvent; Reflux; Inert atmosphere;

Reference yield:

: 544-63-8
n-tetradecanoic acid

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Br₂, HgO red / CCl₄ / 1.5 h / Heating

2: 90 percent / acetonitrile / 24 h / Heating

With bromine; mercury(II) oxide; In tetrachloromethane; acetonitrile;
DOI:10.1016/0040-4020(96)00278-5

Reference yield:

: 112-44-7
undecylaldehyde

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 20 °C

2: 10% Pd/C; hydrogen / ethanol / 20 °C

3: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C

4: carbon tetrabromide / dichloromethane / -30 - 20 °C

5: toluene / Reflux

With lithium aluminium tetrahydride; carbon tetrabromide; 10% Pd/C; hydrogen; In diethyl ether; ethanol; dichloromethane; toluene;
DOI:10.2478/s11696-012-0245-0