dimethyl 3-benzoyl-1-methylthio-1a,7b-dihydrocyclopropanaphthalene-1a,2-dicarboxylate

Base Information

• Chemical Name: dimethyl 3-benzoyl-1-methylthio-1a,7b-dihydrocyclopropa
• Molecular Formula: C₂₃H₂₀O₅S
• Molecular Weight: 408.475

Synonyms:

Chemical Property of dimethyl 3-benzoyl-1-methylthio-1a,7b-dihydrocyclopropa

Chemical Property:

Purity/Quality:

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Useful:

There total 1 articles about dimethyl 3-benzoyl-1-methylthio-1a,7b-dihydrocyclopropanaphthalene-1a,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-benzoyl-2-methyl-1H-2-thianaphthalen-2-ium-1-ide (89805-65-2) + dimethyl acetylenedicarboxylate (762-42-5) → dimethyl 3-benzoyl-1-methylthio-1a,7b-dihydrocyclopropanaphthalene-1a,2-dicarboxylate (78774-74-0)

Guidance literature:

In benzene; at 60 - 70 ℃; for 4h;

DOI:10.1039/c39810000364

upstream raw materials:

1-benzoyl-2-methyl-1H-2-thianaphthalen-2-ium-1-ide

dimethyl acetylenedicarboxylate

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