C₂₂H₃₀O₅

Base Information

Chemical Name:C₂₂H₃₀O₅
CAS No.:1610971-48-6
Molecular Formula:C₂₂H₃₀O₅
Molecular Weight:374.477
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>5</sub>

Synonyms:

Suppliers and Price of C₂₂H₃₀O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₀O₅

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₂H₃₀O₅

There total 13 articles about C₂₂H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610971-47-5
(4S,5R)-4-{[(4-methoxybenzyl)oxy]methyl}-2,2-dimethyl-5-(prop-1-yn-1-yl)-1,3-dioxolane

: 81677-37-4
(E)-tert-butyl(pent-2-en-4-yn-1-yloxy)diphenylsilane

: 1610971-48-6
C₂₂H₃₀O₅

Guidance literature:: C₁₇H₂₂O₄; With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃; Inert atmosphere;

(E)-tert-butyl(pent-2-en-4-yn-1-yloxy)diphenylsilane; In diethyl ether; hexane; toluene; at -78 - -50 ℃; for 3h; Further stages; Inert atmosphere;
DOI:10.1002/ejoc.201301487

Reference yield:

: 1610971-47-5
(4S,5R)-4-{[(4-methoxybenzyl)oxy]methyl}-2,2-dimethyl-5-(prop-1-yn-1-yl)-1,3-dioxolane

: 81677-37-4
(E)-tert-butyl(pent-2-en-4-yn-1-yloxy)diphenylsilane

: 1610971-48-6
C₂₂H₃₀O₅

: C₂₂H₃₀O₅

Guidance literature:: C₁₇H₂₂O₄; With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃; for 2h; Inert atmosphere;

(E)-tert-butyl(pent-2-en-4-yn-1-yloxy)diphenylsilane; In diethyl ether; hexane; toluene; at -78 - -50 ℃; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Overall yield = 64 %; Overall yield = 16.6 mg; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201301487

Reference yield:

: 213767-09-0
2,3-O-isopropylidene-L-erythrofuranose

: 1610971-48-6
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C / Inert atmosphere

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: cyclopentylmagnesium chloride; triisopropoxytitanium(IV) chloride / hexane; diethyl ether; toluene / -78 - -30 °C / Inert atmosphere

4.2: 3 h / -78 - -50 °C / Inert atmosphere

With triisopropoxytitanium(IV) chloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium hydride; cyclopentylmagnesium chloride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201301487