C₄₈H₄₈N₁₀O₇

Base Information

Chemical Name:C₄₈H₄₈N₁₀O₇
CAS No.:1417638-66-4
Molecular Formula:C₄₈H₄₈N₁₀O₇
Molecular Weight:876.972
Hs Code.:

C<sub>48</sub>H<sub>48</sub>N<sub>10</sub>O<sub>7</sub>

Synonyms:

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Chemical Property of C₄₈H₄₈N₁₀O₇

Chemical Property:

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Technology Process of C₄₈H₄₈N₁₀O₇

There total 8 articles about C₄₈H₄₈N₁₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19872-91-4
dimethyl 4-hydroxypyridine-2,6-dicarboxylate

: 1417638-66-4
C₄₈H₄₈N₁₀O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydroxide; water / methanol

3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 0 - 20 °C

3.2: 1 h / 0 - 20 °C

4.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

4.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

With copper(ll) sulfate pentahydrate; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; di-isopropyl azodicarboxylate; water; sodium L-ascorbate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201206281

Reference yield:

: 499-51-4
Chelidamic acid

: 1417638-66-4
C₄₈H₄₈N₁₀O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / -10 °C / Reflux

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide; water / methanol

4.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

5.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

With thionyl chloride; copper(ll) sulfate pentahydrate; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; di-isopropyl azodicarboxylate; water; sodium L-ascorbate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201206281

Reference yield:

: 2-aminoquinolin-4-one

: 1417638-66-4
C₄₈H₄₈N₁₀O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

2.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / dichloromethane / 2 h / 0 - 20 °C

2.2: 1 h / 0 - 20 °C

3.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 0.17 h / Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

3.2: Inert atmosphere; Combinatorial reaction / High throughput screening (HTS)

With copper(ll) sulfate pentahydrate; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; di-isopropyl azodicarboxylate; sodium L-ascorbate; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1002/anie.201206281