4'-(2-methyl-1-butoxy)benzylcyanide

Base Information

• Chemical Name: 4'-(2-methyl-1-butoxy)benzylcyanide
• CAS No.: 845511-23-1
• Molecular Formula: C₁₃H₁₇NO
• Molecular Weight: 203.284
• Mol file: 845511-23-1.mol

Synonyms:

Chemical Property of 4'-(2-methyl-1-butoxy)benzylcyanide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4'-(2-methyl-1-butoxy)benzylcyanide

There total 1 articles about 4'-(2-methyl-1-butoxy)benzylcyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-cyanomethylphenol (14191-95-8) + p-toluenesulfonic acid 2-methylbutyl ester (63526-71-6) → 4'-(2-methyl-1-butoxy)benzylcyanide (845511-23-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 4h;

DOI:10.1080/15421400490478326

Reference yield:

4-methoxymethoxy-benzaldehyde (6515-21-5) + 4'-(2-methyl-1-butoxy)benzylcyanide (845511-23-1) → (Z)-3-(4-Methoxymethoxy-phenyl)-2-[4-(2-methyl-butoxy)-phenyl]-acrylonitrile

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 4h;

DOI:10.1080/15421400490478326

Reference yield:

4'-(2-methyl-1-butoxy)benzylcyanide (845511-23-1) → 4-(2-methylbutoxy)-4'-hydroxycyanostilbene (845511-26-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 4 h / 20 °C

2: aq. HCl / methanol; tetrahydrofuran / 12 h / 50 °C

With hydrogenchloride; potassium hydroxide; In tetrahydrofuran; methanol; ethanol;

DOI:10.1080/15421400490478326

upstream raw materials:

4-cyanomethylphenol

p-toluenesulfonic acid 2-methylbutyl ester

Downstream raw materials:

4-(2-methylbutoxy)-4'-hydroxycyanostilbene