3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.1^5,9.1^13,17.1^21,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene

Base Information

• Chemical Name: 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.1^5,9.1^13,17.1^21,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene
• CAS No.: 125683-06-9
• Molecular Formula: C₅₆H₅₆N₈O₈S₄
• Molecular Weight: 1097.37

Synonyms:

Chemical Property of 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.1^5,9.1^13,17.1^21,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene

Chemical Property:

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Technology Process of 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.1^5,9.1^13,17.1^21,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene

There total 6 articles about 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.1^5,9.1^13,17.1^21,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

C21H21N3O4S2(2-)*2Na(1+) + 2,6-bis<pyridin-2-yl>methyl>-N-tosylamino>methyl>pyridine (125683-03-6) → 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.15,9.113,17.121,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene (125683-06-9)

Guidance literature:

In N,N-dimethyl-formamide; at 90 ℃; for 3h;

DOI:10.1002/hlca.19890720525

Reference yield:

2,6-bis(aminomethyl)pyridine (34984-16-2) → 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.15,9.113,17.121,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene (125683-06-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent

2: Na / methanol / 2 h / Heating

3: 35 percent / dimethylformamide / 3 h / 90 °C

With sodium; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

Reference yield:

2,6-bis<(p-tosylamino)methyl>pyridine (112633-27-9) → 3,11,19,27-tetratosyl-3,11,19,27,33,34,35,36-octaazapentacyclo<27.3.1.15,9.113,17.121,25>hexatriaconta-1(33),5(34),6,8,13(35),14,16,21(36),22,24,29,31-dodecaene (125683-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Na / methanol / 2 h / Heating

2: 35 percent / dimethylformamide / 3 h / 90 °C

With sodium; In methanol; N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

upstream raw materials:

2,6-bis<pyridin-2-yl>methyl>-N-tosylamino>methyl>pyridine

2,6-bis(aminomethyl)pyridine

2,6-bis<(p-tosylamino)methyl>pyridine

p-toluenesulfonyl chloride

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