2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

Base Information

Chemical Name:2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine
CAS No.:162894-91-9
Molecular Formula:C₅₁H₄₉N₃O₁₈S₂
Molecular Weight:1056.09
Hs Code.:

2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

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Chemical Property of 2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

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Technology Process of 2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

There total 8 articles about 2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 162894-83-9
O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl) trichloroacetimidate

: 162894-90-8
2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-β-D-glucopyranosylamine

: 162894-91-9
2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; In dichloromethane; for 1.5h; Ambient temperature;
DOI:10.1039/P19950000405

Reference yield:

: 29847-23-2
2-N-acetylamido-2-deoxy-β-D-glucopyranosyl azide

: 162894-91-9
2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 67.7 percent / pyridine / CH₂Cl₂ / 3 h / -45 °C

2: H₂ / Pd/C / methanol / 2 h

3: Ambient temperature

4: 47 percent / molecular sieves 3A, TMSOTf / CH₂Cl₂ / 1.5 h / Ambient temperature

With pyridine; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1039/P19950000405

Reference yield:

: 98-88-4
benzoyl chloride

: 162894-91-9
2-acetamido-3,6-di-O-benzoyl-2-deoxy-N-(fluoren-9-ylmethoxycarbonyl)-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl)-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 67.7 percent / pyridine / CH₂Cl₂ / 3 h / -45 °C

2: H₂ / Pd/C / methanol / 2 h

3: Ambient temperature

4: 47 percent / molecular sieves 3A, TMSOTf / CH₂Cl₂ / 1.5 h / Ambient temperature

With pyridine; trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1039/P19950000405