[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

Base Information

Chemical Name:[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2
CAS No.:1221071-52-8
Molecular Formula:C₈₈H₁₀₄N₄O₁₀Pd₂
Molecular Weight:1590.65
Hs Code.:

[Pd(NCC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6OC<sub>6</sub>H<sub>3</sub>CHNC<sub>6</sub>H<sub>4</sub>OC<sub>10</sub>H<sub>21</sub>)(CH<sub>3</sub>COO)]2

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Chemical Property of [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

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Technology Process of [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

There total 1 articles about [Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1221071-67-5
NCC₆H₄C₆H₄O(CH₂)6OC₆H₄CHNC₆H₄OC₁₀H₂₁

: 3375-31-3
palladium diacetate

: 1221071-52-8
[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

Guidance literature:: In acetic acid; Schiff base and palladium acetate in glacial acetic acid heated under reflux for 7 h; ppt. filtered hot and washed several times with acetic acid; recrystd. from CH2Cl2/C2H5OH at -25°C; elem. anal.;
DOI:10.1016/j.ica.2009.11.028

Reference yield: 85.0%

: N,N-di-n-butyl-N'-benzoyl thiourea sodium salt

: 1221071-52-8
[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

: 1221071-58-4
[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-dibutyl-N'-benzoyl thiourea)]

Guidance literature:: In dichloromethane; Na(C6H5CONSONBu2) salt added to soln. of binuclear complex of Pd in CH2Cl2; mixt. stirred at room temp. for 1 d and then solvent removed; residue purified on silica using CH2Cl2 as eluent; complex recrystd. from CH2Cl2/C2H5OH at -25°C; elem. anal.;
DOI:10.1016/j.ica.2009.11.028

Reference yield: 79.0%

: N,N-diethyl-N'-benzoyl thiourea sodium salt

: 1221071-52-8
[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(CH₃COO)]2

: 1221071-54-0
[Pd(NCC₆H₄C₆H₄O(CH₂)6OC₆H₃CHNC₆H₄OC₁₀H₂₁)(N,N-diethyl-N'-benzoyl thiourea)]

Guidance literature:: In dichloromethane; Na(C6H5CONSONEt2) salt added to soln. of binuclear complex of Pd in CH2Cl2; mixt. stirred at room temp. for 1 d and then solvent removed; residue purified on silica using CH2Cl2 as eluent; complex recrystd. from CH2Cl2/C2H5OH at -25°C; elem. anal.;
DOI:10.1016/j.ica.2009.11.028