mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III)

Base Information

Chemical Name:mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III)
CAS No.:136244-48-9
Molecular Formula:C₁₈H₃₅Cl₃OP₃V
Molecular Weight:517.697
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III)

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Technology Process of mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III)

There total 1 articles about mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 136210-98-5
trans,mer-trichlorobis(dimethylphenylphosphine)(dimethylphenylphosphine oxide-κO)vanadium(III)

: 6411-21-8
depe

: 136244-48-9
mer-{1,2-bis(diethylphosphino)ethane}trichloro(dimethylphenylphosphine oxide-κO)vanadium(III)

Guidance literature:: In toluene; under N2, 1 h stirring, rapid colour change to green; solvent removed in vac., resulting oil dissolved in min. of CH2Cl2, addn. of large excess of hexane, leaving at -20°C for 3 d, elem. anal.;
DOI:10.1039/DT9910001755