C₂₅H₂₄O₇S

Base Information

Chemical Name:C₂₅H₂₄O₇S
CAS No.:1438868-44-0
Molecular Formula:C₂₅H₂₄O₇S
Molecular Weight:468.527
Hs Code.:

C<sub>25</sub>H<sub>24</sub>O<sub>7</sub>S

Synonyms:

Suppliers and Price of C₂₅H₂₄O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₄O₇S

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₅H₂₄O₇S

There total 13 articles about C₂₅H₂₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₈O₃S

: 1438868-44-0
C₂₅H₂₄O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N,N-dimethyl-formamide / 25 °C / Inert atmosphere

2.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

3.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux

6.1: toluene-4-sulfonic acid / 1 h / 20 °C / Inert atmosphere; Reflux

7.1: alkaline hydroxide / 12 h / Inert atmosphere; Reflux

7.2: pH 3-4 / Inert atmosphere

With hydrogenchloride; dmap; water; copper; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977

Reference yield:

: C₁₉H₂₂O₃S

: 1438868-44-0
C₂₅H₂₄O₇S

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

2.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

3.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux

4.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / 1 h / 20 °C / Inert atmosphere; Reflux

6.1: alkaline hydroxide / 12 h / Inert atmosphere; Reflux

6.2: pH 3-4 / Inert atmosphere

With hydrogenchloride; dmap; water; copper; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977

Reference yield:

: C₂₈H₃₂O₈S

: 1438868-44-0
C₂₅H₂₄O₇S

Guidance literature:: C₂₈H₃₂O₈S; for 12h; Inert atmosphere; Reflux;

With hydrogenchloride; In water; pH=3-4; Inert atmosphere;
DOI:10.1002/cjoc.201200977