cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate

Base Information

Chemical Name:cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate
CAS No.:86614-56-4
Molecular Formula:C₂₇H₂₆NPS₂
Molecular Weight:459.616
Hs Code.:

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Chemical Property of cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate

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Technology Process of cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate

There total 1 articles about cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 626-62-0
Cyclohexyl iodide

: 14652-29-0
Cyano-(triphenyl-λ⁵-phosphanylidene)-dithioacetic acid; compound with triethyl-amine

: 86614-56-4
cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate

Guidance literature:: for 24h;
DOI:10.1016/0022-328X(83)85026-8

Reference yield: 50.0%

: 14040-11-0
tungsten hexacarbonyl

: 86614-56-4
cyclohexyl 2-cyano-2-triphenylphosphoranylidene dithioacetate

: pentacarbonyl[cyclohexyl (2-cyano-2-triphenylphosphoranylidenedithioacetate)]tungsten⁽⁰⁾

Guidance literature:: In not given; Irradiation (UV/VIS); ligand mixed at room temp. with irradiated complex (excess), reacted for 20-30 min; solvent removed, residue chromd. (SiO2, n-hexane/CH2Cl2/EtOAc), cooled,decanted, washed with EtOAc, then with n-hexane, dried (vac.); elem. anal.;
DOI:10.1016/0022-328X(83)85026-8