C₂₆H₂₆N₂O₂

Base Information

• Chemical Name: C₂₆H₂₆N₂O₂
• CAS No.: 85678-99-5
• Molecular Formula: C₂₆H₂₆N₂O₂
• Molecular Weight: 398.505
• Mol file: 85678-99-5.mol

Synonyms:

Chemical Property of C₂₆H₂₆N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₆N₂O₂

There total 5 articles about C₂₆H₂₆N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2-<2-(1-methoxynaphthyl)>-4,4-dimethyl-Δ2-oxazoline (78265-10-8) + 2-(2-lithiophenyl)-4,4-dimethyl-Δ2-oxazoline (66464-21-9) → C26H26N2O2 (85678-99-5)

Guidance literature:

In tetrahydrofuran; diethyl ether; at -15 - 0 ℃; for 1.5h;

DOI:10.1055/s-1983-30235

Reference yield:

1-methoxy-2-naphthoic acid (883-21-6) → C26H26N2O2 (85678-99-5)

Guidance literature:

Multi-step reaction with 5 steps

1: oxalyl chloride / CH₂Cl₂ / 18 h / 0 deg C -> room temp.

2: CH₂Cl₂ / 18 h / Ambient temperature

3: thionyl chloride / 0.5 h / Ambient temperature

4: 20percent aq. NaOH

5: 32 percent / tetrahydrofuran; diethyl ether / 1.5 h / -15 - 0 °C

With sodium hydroxide; thionyl chloride; oxalyl dichloride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1055/s-1983-30235

Reference yield:

1-methoxy-2-naphthoyl chloride (51439-63-5) → C26H26N2O2 (85678-99-5)

Guidance literature:

Multi-step reaction with 4 steps

1: CH₂Cl₂ / 18 h / Ambient temperature

2: thionyl chloride / 0.5 h / Ambient temperature

3: 20percent aq. NaOH

4: 32 percent / tetrahydrofuran; diethyl ether / 1.5 h / -15 - 0 °C

With sodium hydroxide; thionyl chloride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1055/s-1983-30235

upstream raw materials:

2-<2-(1-methoxynaphthyl)>-4,4-dimethyl-Δ²-oxazoline

2-(2-lithiophenyl)-4,4-dimethyl-Δ²-oxazoline

1-methoxy-2-naphthoic acid

1-methoxy-2-naphthoyl chloride

Downstream raw materials:

1-(2'-Carboxyphenyl)-2-naphthoic acid