Technology Process of C21H22ClN5O3S*ClH
There total 8 articles about C21H22ClN5O3S*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere
1.2: 3 h / 20 °C / Inert atmosphere
2.1: hydroxylamine hydrochloride / ethanol / 6 h / Reflux
3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 4 h / 0 °C
4.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 24 h / 20 °C
5.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 20 °C
5.2: 4 h / 20 °C
6.1: hydrogenchloride / chloroform / 0.5 h / 0 °C
7.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 25 h / 0 - 20 °C
8.1: hydrogenchloride / chloroform / 0.5 h / 0 °C
With
hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; hydroxylamine hydrochloride; sodium hydride; triethylamine; triphenylphosphine; mercury dichloride;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 25 h / 0 - 20 °C
2: hydrogenchloride / chloroform / 0.5 h / 0 °C
With
hydrogenchloride; triethylamine; mercury dichloride;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejps.2010.11.010
