<7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

Base Information

Chemical Name:<7-(1-Aminocyclopropanecarboxylic acid)>oxytocin
CAS No.:88463-32-5
Molecular Formula:C₄₂H₆₄N₁₂O₁₂S₂
Molecular Weight:993.175
Hs Code.:

Synonyms:

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Chemical Property of <7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

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Technology Process of <7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

There total 9 articles about <7-(1-Aminocyclopropanecarboxylic acid)>oxytocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Cysteinyl-tyrosyl-isoleucyl-glutaminyl-aparaginyl-cystein-1-aminocyclopropane-1-carboxy-leucyl-glycine Amide

: 88463-32-5
<7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

Guidance literature:: With potassium hexacyanoferrate(III); In water; for 0.583333h; Ambient temperature; pH = 7;
DOI:10.1135/cccc19840642

Reference yield:

: 2867-06-3
Benzyloxycarbonylleucyl-glycine ethyl ester

: 88463-32-5
<7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

Guidance literature:: Multi-step reaction with 7 steps

1: HBr / acetic acid

2: 350 mg / dicyclohexylcarbodiimide / CHCl₃ / 1) -10 deg C, 1 h, 2) 0 deg C, overnight

3: 61 percent / ammonia / methanol / 96 h / Ambient temperature

4: hydrobromic acid / acetic acid; H₂O / 0.5 h / Ambient temperature

5: 68 mg / 1) 1-hydroxybenzotriazole, 2) dicyclohexylcarbodiimide, N-ethylpiperidine / dimethylformamide / 1) Room temp. 2) -20 deg C, 1 h, 3) room temp. overnight

6: liquid hydrogen fluoride, anisole / 1 h / 20 °C

7: 1.52 mg / K₃Fe(CN)6 / H₂O / 0.58 h / Ambient temperature; pH = 7

With 1-ethyl-piperidine; hydrogen fluoride; ammonia; hydrogen bromide; benzotriazol-1-ol; methoxybenzene; dicyclohexyl-carbodiimide; potassium hexacyanoferrate(III); In methanol; chloroform; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1135/cccc19840642

Reference yield:

: 88463-37-0
Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-aparaginyl-S-benzylcystein-1-aminocyclopropane-1-carboxy-leucyl-glycine Amide

: 88463-32-5
<7-(1-Aminocyclopropanecarboxylic acid)>oxytocin

Guidance literature:: Multi-step reaction with 2 steps

1: liquid hydrogen fluoride, anisole / 1 h / 20 °C

2: 1.52 mg / K₃Fe(CN)6 / H₂O / 0.58 h / Ambient temperature; pH = 7

With hydrogen fluoride; methoxybenzene; potassium hexacyanoferrate(III); In water;
DOI:10.1135/cccc19840642