Technology Process of C28H31N5O4
There total 3 articles about C28H31N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium tert-butylate / tert-butyl alcohol
2: palladium on activated charcoal; hydrogen / methanol; ethyl acetate
3: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
With
palladium on activated charcoal; potassium tert-butylate; hydrogen; triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one;
In
methanol; dichloromethane; ethyl acetate; tert-butyl alcohol;
1: Stobbe condensation;
DOI:10.1016/j.bmcl.2012.02.066
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; hydrogen / methanol; ethyl acetate
2: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
With
palladium on activated charcoal; hydrogen; triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2012.02.066
- Guidance literature:
-
With
triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one;
In
dichloromethane;
DOI:10.1016/j.bmcl.2012.02.066
