1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

Base Information

Chemical Name:1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol
CAS No.:1384424-18-3
Molecular Formula:C₅₁H₇₆F₈N₂O₉
Molecular Weight:1013.16
Hs Code.:

1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

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Chemical Property of 1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

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Technology Process of 1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

There total 13 articles about 1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1384424-18-3
1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

Guidance literature:

Reference yield:

: 1384424-12-7
1-O-(6-amino-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

: 1384424-19-4
C₁₀H₆F₆O₂

: 1384424-18-3
1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

Guidance literature:: With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/cbic.201200004

Reference yield:

: 2-amino-3,4-di-O-benzyl-1-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-D-ribo-octadecane-1,3,4-triol

: 1384424-18-3
1-O-(6-(3,4-di(trifluoromethyl)phenyl-acetamido)-6-deoxy-α-D-galactopyranosyl)-2-(11-(3,4-difluorophenyl)undecanoyl)amino-D-ribo-1,3,4-octadecanetriol

Guidance literature:: Multi-step reaction with 6 steps

1: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 12 h / 20 °C

2: hydrogen; palladium(II) hydroxide / methanol; dichloromethane / 12 h / 20 °C

3: pyridine / 16 h / 0 - 20 °C

4: sodium azide / N,N-dimethyl-formamide / 48 h / 100 °C

5: water; triphenylphosphine / tetrahydrofuran / 48 h / 20 °C

6: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / methanol; dichloromethane / 16 h / 20 °C

With 4-methyl-morpholine; pyridine; sodium azide; water; hydrogen; palladium(II) hydroxide; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 5: Staudinger reaction;
DOI:10.1002/cbic.201200004