5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid
CAS No.:127743-84-4
Molecular Formula:C₇H₈O₃S*C₁₇H₂₁N₅O₅
Molecular Weight:547.589
Hs Code.:

5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

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Chemical Property of 5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

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Technology Process of 5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

There total 4 articles about 5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 127743-84-4
5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / K₂CO₃ / dimethylformamide / 30 h / Ambient temperature

2: H₂ / Raney Ni / H₂O; ethanol / 6 h / Ambient temperature

With hydrogen; potassium carbonate; nickel; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.3200

Reference yield:

: 1-benzyloxyadenosine perchlorate monohydrate

: 127743-84-4
5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 10percent NaOH / H₂O / 4 h / 40 °C / pH 9.5

2: 66 percent / K₂CO₃ / dimethylformamide / 30 h / Ambient temperature

3: H₂ / Raney Ni / H₂O; ethanol / 6 h / Ambient temperature

With sodium hydroxide; hydrogen; potassium carbonate; nickel; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.3200

Reference yield:

: 50507-48-7
N'-benzyloxy-5-formamido-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine

: 127743-84-4
5-(Benzyl-formyl-amino)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxamidine; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / K₂CO₃ / dimethylformamide / 30 h / Ambient temperature

2: H₂ / Raney Ni / H₂O; ethanol / 6 h / Ambient temperature

With hydrogen; potassium carbonate; nickel; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.3200