IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

Base Information

Chemical Name:IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃
CAS No.:100857-91-8
Molecular Formula:CHCl₃*C₅₅H₄₄Cl₂F₆IrOP₄Rh
Molecular Weight:1503.94
Hs Code.:

IrCl(CO)RhCl(CF<sub>3</sub>C<sub>2</sub>CF<sub>3</sub>)(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)2*1.5CHCl<sub>3</sub>

Synonyms:

Suppliers and Price of IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

There total 1 articles about IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87482-56-2
IrRhCl(CO)3(((C₆H₅)2P)2CH₂)2

: 922-67-8
propynoic acid methyl ester

: 100857-91-8
IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

Guidance literature:: With carbon monoxide; In tetrahydrofuran; dichloromethane; pressurizing complex in CO-satd. solvent with ligand and CO, stirring for 0.5 h, filtering through diatomaceous earth, addn. of Et2O, filteringoff, refluxing of the solid in THF under N2 purge for 5 h; filtn. through diatomaceous earth, addn. of Et2O, filtn., recrystallization from CHCl3-Et2O; elem. anal.;
DOI:10.1021/om00136a014

Reference yield:

: 100857-91-8
IrCl(CO)RhCl(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*1.5CHCl₃

: IrCl(CO)RhCl(CO)(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2

: 100815-18-7
IrCl(CO)RhCl(CO)(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2*3CHCl₃

: IrCl(CO)RhCl(CO)(CF₃C₂CF₃)(((C₆H₅)2P)2CH₂)2

Guidance literature:: With carbon monoxide; In chloroform; CO was purged through soln. of complex, color changed rapidly from burgundy to bright yellow; pptn. on standing, collecting, washing with Et2O, drying in vacuo, elem. anal., IR;
DOI:10.1021/om00136a014