3-phenylcarbamoylbenzhydroxamic acid

Base Information

• Chemical Name: 3-phenylcarbamoylbenzhydroxamic acid
• CAS No.: 1440210-02-5
• Molecular Formula: C₁₄H₁₂N₂O₃
• Molecular Weight: 256.261
• Mol file: 1440210-02-5.mol

Synonyms:

Chemical Property of 3-phenylcarbamoylbenzhydroxamic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenylcarbamoylbenzhydroxamic acid

There total 4 articles about 3-phenylcarbamoylbenzhydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H20N2O4 → 3-phenylcarbamoylbenzhydroxamic acid (1440210-02-5)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1021/acs.jmedchem.7b01447

Reference yield:

3-methoxycarbonyl-N-phenylbenzamide (139191-85-8) → 3-phenylcarbamoylbenzhydroxamic acid (1440210-02-5)

Guidance literature:

With hydroxylamine; sodium hydroxide; In methanol; dichloromethane; water;

DOI:10.1021/jm400390r

Reference yield:

3-(phenylcarbamoyl)benzoic acid (16776-94-6) → 3-phenylcarbamoylbenzhydroxamic acid (1440210-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran

2: hydrogenchloride / tetrahydrofuran; water / 20 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water;

DOI:10.1021/acs.jmedchem.7b01447

upstream raw materials:

benzene 1,3-dicarboxylic acid monomethyl ester

aniline

3-methoxycarbonyl-N-phenylbenzamide

3-(phenylcarbamoyl)benzoic acid