C₁₃H₁₃F₃N₄

Base Information

Chemical Name:C₁₃H₁₃F₃N₄
CAS No.:1262197-60-3
Molecular Formula:C₁₃H₁₃F₃N₄
Molecular Weight:282.268
Hs Code.:

C<sub>13</sub>H<sub>13</sub>F<sub>3</sub>N<sub>4</sub>

Synonyms:

Suppliers and Price of C₁₃H₁₃F₃N₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₃H₁₃F₃N₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₃H₁₃F₃N₄

There total 4 articles about C₁₃H₁₃F₃N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262198-08-2
8-(2-(trifluoromethyl)phenyl)-[1,2,4]triazolo[1,5-a]pyridin-2-amine

: 1262197-60-3
C₁₃H₁₃F₃N₄

Guidance literature:: With hydrogenchloride; palladium on activated charcoal; In methanol; isopropyl alcohol; at 50 ℃; for 16h;
DOI:10.1016/j.bmcl.2013.06.100

Reference yield:

: 13534-99-1
2-Amino-3-bromopyridine

: 1262197-60-3
C₁₃H₁₃F₃N₄

Guidance literature:: Multi-step reaction with 4 steps

1: 1,4-dioxane / 12 h / 20 °C

2: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / methanol

3: sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.17 h / 150 °C / Microwave irradiation

4: palladium on activated charcoal; hydrogenchloride / methanol; isopropyl alcohol / 16 h / 50 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; hydroxylamine hydrochloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; isopropyl alcohol; 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2013.06.100

Reference yield:

: 1124383-00-1
N-(3-bromo-2-pyridinyl)-N’-carboethoxy-thiourea

: 1262197-60-3
C₁₃H₁₃F₃N₄

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / methanol

2: sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,4-dioxane / 0.17 h / 150 °C / Microwave irradiation

3: palladium on activated charcoal; hydrogenchloride / methanol; isopropyl alcohol / 16 h / 50 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; hydroxylamine hydrochloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; isopropyl alcohol; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2013.06.100