Technology Process of (E,E,E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl 4-nitrobenzoate
There total 1 articles about (E,E,E)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl 4-nitrobenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
for 18h;
Ambient temperature;
-
-
131265-63-9,131347-63-2
(+/-)-1-<2,5-bis(methoxymethoxy)-3-methylbenzyl>-1,2-epoxy-1,2,3,4,4aα,4b,5,6,7,8,8aα,9,10,10a-tetradecahydro-2,4bβ,8,8,10aβ-pentamethylphenanthrene
- Guidance literature:
-
Multi-step reaction with 6 steps
2: PCC, NaOAc / CH2Cl2 / 2.5 h / Ambient temperature
3: 86 percent / NaBH4 / methanol; hexane / 0.83 h / 0 °C
4: 95 percent / (CClBr2)2, PPh3 / diethyl ether / 1.5 h / 0 °C
6: 71 percent / MCPBA / CH2Cl2 / 16 h / Ambient temperature
With
sodium tetrahydroborate; tetrabromo-1,2-dichloro-ethane; sodium acetate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate;
In
methanol; diethyl ether; hexane; dichloromethane;
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-
131273-43-3
(+/-)-1-<2,5-bis(methoxymethoxy)-3-methylbenzyl>-3,4,4aα,5,6,7,8,8aα,9,10,10a-dodecahydro-2,4bβ,8,8,10aβ-pentamethylphenanthrene
- Guidance literature:
-
Multi-step reaction with 5 steps
2: PCC, NaOAc / CH2Cl2 / 2.5 h / Ambient temperature
3: 86 percent / NaBH4 / methanol; hexane / 0.83 h / 0 °C
4: 95 percent / (CClBr2)2, PPh3 / diethyl ether / 1.5 h / 0 °C
With
sodium tetrahydroborate; tetrabromo-1,2-dichloro-ethane; sodium acetate; triphenylphosphine; pyridinium chlorochromate;
In
methanol; diethyl ether; hexane; dichloromethane;
