(+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole

Base Information

Chemical Name:(+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole
CAS No.:133056-49-2
Molecular Formula:C₂₄H₂₅NO₅
Molecular Weight:407.466
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole

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Technology Process of (+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole

There total 3 articles about (+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123796-58-7
1,4,5-Trimethoxynaphthalene-2-carbonitrile

: 133056-49-2
(+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / potassium hydroxide / 2-methyl-propan-2-ol / 1.5 h / Heating

2: 1.) triethyloxonium tetrafluoroborate / 1.) 1,2-dichloroethane, r.t., 24h, 2.) reflux, 48h

With potassium hydroxide; triethyloxonium fluoroborate; In tert-butyl alcohol;
DOI:10.1039/P19910000845

Reference yield:

: 51594-34-4
(1S,2S)-2-amino-3-methoxy-1-phenyl-1-propanol

: 133056-48-1
1,4,5-Trimethoxynaphthalene-2-carboxamide

: 133056-49-2
(+)-(4S,5S)-4-(Methoxymethyl)-5-phenyl-2-(1,4,5-trimethoxy-2-naphthyl)-4,5-dihydroxooxazole

Guidance literature:: With triethyloxonium fluoroborate; Yield given. Multistep reaction; 1.) ClCH₂CH₂Cl, 25 deg C, 24 h, 2.) reflux, 48 h;
DOI:10.1039/c39900000894