(Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: (Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 118645-99-1
• Molecular Formula: C₃₇H₅₉F₄NO₂
• Molecular Weight: 625.875

Synonyms:

Chemical Property of (Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 2 articles about (Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) + 3β-cholestanyl 2H-perfluorobutanoate (97509-97-2,123613-17-2,127420-75-1,127420-78-4) → (Z)-3-Cyclohexylamino-2,4,4,4-tetrafluoro-but-2-enoic acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (118645-99-1) + 3-[(Z)-Cyclohexylimino]-2,4,4,4-tetrafluoro-butyric acid (3S,8R,9S,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (118645-98-0,118646-12-1)

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 24h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)82153-X

Reference yield:

α-hydroperfluorobutanoate de cholestanyle (97509-97-2) + cyclohexylamine (108-91-8,157973-60-9) → 3-cyclohexylamino-2,4,4,4-tetrafluorobut-2-enoate de cholestanyle (118645-99-1) + 3-cyclohexylimino-2,4,4,4-tetrafluorobutanoate de cholestanyle

Guidance literature:

In tetrahydrofuran; for 24h; Yield given. Yields of byproduct given; Heating;

DOI:10.1016/S0022-1139(00)80302-4

upstream raw materials:

α-hydroperfluorobutanoate de cholestanyle

cyclohexylamine

3β-cholestanyl 2H-perfluorobutanoate

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