C₄₄H₄₆ClN₃O₁₃

Base Information

Chemical Name:C₄₄H₄₆ClN₃O₁₃
CAS No.:1398047-55-6
Molecular Formula:C₄₄H₄₆ClN₃O₁₃
Molecular Weight:860.315
Hs Code.:

C<sub>44</sub>H<sub>46</sub>ClN<sub>3</sub>O<sub>13</sub>

Synonyms:

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Chemical Property of C₄₄H₄₆ClN₃O₁₃

Chemical Property:

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Technology Process of C₄₄H₄₆ClN₃O₁₃

There total 7 articles about C₄₄H₄₆ClN₃O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1398044-77-3
4-methoxyphenyl 4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranoside

: 1398047-55-6
C₄₄H₄₆ClN₃O₁₃

: 1398044-82-0
C₄₄H₄₆ClN₃O₁₃

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃;
DOI:10.1002/chem.201204519

Reference yield:

: C₂₆H₂₇N₃O₄S

: 1398047-55-6
C₄₄H₄₆ClN₃O₁₃

: 1398044-82-0
C₄₄H₄₆ClN₃O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

2.1: acetic acid / water / 8 h / 80 °C

3.1: pyridine / 6 h / 20 °C

4.1: toluene; dichloromethane / 0.17 h / -15 °C / Molecular sieve

4.2: 1 h / 20 °C / Molecular sieve

5.1: ammonium cerium (IV) nitrate / water; acetonitrile / 20 °C

With pyridine; ammonium cerium (IV) nitrate; sodium hydride; acetic acid; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201204519

Reference yield:

: 1398044-64-8
methyl 2-azido-3,4-di-O-benzyl-2-deoxy-1-thio-6-O-trityl-β-D-glucopyranoside

: 1398047-55-6
C₄₄H₄₆ClN₃O₁₃

: 1398044-82-0
C₄₄H₄₆ClN₃O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / water / 8 h / 80 °C

2.1: pyridine / 6 h / 20 °C

3.1: toluene; dichloromethane / 0.17 h / -15 °C / Molecular sieve

3.2: 1 h / 20 °C / Molecular sieve

4.1: ammonium cerium (IV) nitrate / water; acetonitrile / 20 °C

With pyridine; ammonium cerium (IV) nitrate; acetic acid; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/chem.201204519