12-methyldodecalactone

Base Information

Chemical Name:12-methyldodecalactone
CAS No.:69297-53-6
Molecular Formula:C₁₃H₂₄O₂
Molecular Weight:212.332
Hs Code.:

Synonyms:

Suppliers and Price of 12-methyldodecalactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12-methyldodecalactone

Chemical Property:

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Technology Process of 12-methyldodecalactone

There total 1 articles about 12-methyldodecalactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 830-13-7
cyclododecanone

: 74-88-4
methyl iodide

: 1725-03-7
oxacyclododecan-2-one

: 69297-53-6,88785-33-5,71736-24-8
12-methyldodecalactone

Guidance literature:: cyclododecanone; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; hexane; at -78 ℃;

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 70 ℃; for 168000h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ja071241a

Reference yield:

: 69297-53-6,88785-33-5,71736-24-8
12-methyldodecalactone

: 100-51-6,185532-71-2
benzyl alcohol

: C₂₀H₃₂O₃

Guidance literature:: Novozym 435; In toluene; at 70 ℃; Enzyme kinetics;
DOI:10.1021/ja071241a

Reference yield:

: 69297-53-6,88785-33-5,71736-24-8
12-methyldodecalactone

: 1393825-30-3
(R)-(12-azidotridecyloxy)triphenylmethane

Guidance literature:: Multi-step reaction with 5 steps

1: Candida antarctica lipase B / toluene / 70 °C / Inert atmosphere; Enzymatic reaction

2: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C / Inert atmosphere

3: pyridine; dmap / 60 h / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

5: sodium azide / N,N-dimethyl-formamide / 60 °C / Inert atmosphere

With pyridine; dmap; Candida antarctica lipase B; lithium aluminium tetrahydride; sodium azide; triethylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2012.05.021