Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-

Base Information

Chemical Name:Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-
CAS No.:930765-00-7
Molecular Formula:C₁₄H₉F₆PS₂
Molecular Weight:386.322
Hs Code.:

Synonyms:Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-

Suppliers and Price of Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]-

There total 2 articles about Phosphinodithioic acid, P,P-bis[2-(trifluoromethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₁₆F₁₂NiP₂S₄

: 930765-00-7
bis(o-trifluoromethylphenyl)dithiophosphinic acid

Guidance literature:: With hydrogenchloride; In water; at 20 ℃;
DOI:10.1021/acs.inorgchem.8b01635

Reference yield:

: C₁₄H₈ClF₆PS

: 930765-00-7
bis(o-trifluoromethylphenyl)dithiophosphinic acid

Guidance literature:: With sodium hydrogen sulfide; In diethyl ether; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.inorgchem.8b01635

Reference yield: 70.0%

: 930765-00-7
bis(o-trifluoromethylphenyl)dithiophosphinic acid

: 83864-14-6
nickel dichloride

: 1384253-23-9
bis[bis(o-trifluoromethylphenyl)dithiophosphinato]nickel(II)

Guidance literature:: In ethanol; water; soln. ligand in EtOH was added to soln. NiCl2 in water, stirred at room temp. for 3 h; soln. was filtered, washed with water and EtOH and allowed to evaporate in air, residue was dissolved in CH2Cl2-hexane (8:1), slow evapn.; elem.anal.;
DOI:10.1021/ic3001587