diphenyl (2-thienyl)phosphine selenide

Base Information

Chemical Name:diphenyl (2-thienyl)phosphine selenide
CAS No.:79133-89-4
Molecular Formula:C₁₆H₁₃PSSe
Molecular Weight:347.279
Hs Code.:

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Chemical Property of diphenyl (2-thienyl)phosphine selenide

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Technology Process of diphenyl (2-thienyl)phosphine selenide

There total 1 articles about diphenyl (2-thienyl)phosphine selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61157-16-2
diphenyl(2-thienyl)phosphine

: 79133-89-4
diphenyl (2-thienyl)phosphine selenide

Guidance literature:: With selenium; In chloroform; for 5h; Heating;
DOI:10.1039/DT9820000051

Reference yield: 30.0%

: HRuCo₃*12CO=HRuCo₃(CO)12

: 79133-89-4
diphenyl (2-thienyl)phosphine selenide

: (RuCo2(μ3-Se)(CO)8(dpth))

: (RuCo2(μ3-Se)(CO)7(dpth)2)

: (HRuCo3(CO)8(μ-CO)3(dpth))

Guidance literature:: In toluene; under N2 atm. (HRuCo3(CO)12) was treated with dpthSe in toluene at 70°C for 2 h; soln. was evapd. to dryness, residue was dissolved in CH2Cl2, TLC on silica using CH2Cl2-hexane (1:1) as eluent; elem. anal.;
DOI:10.1021/ic010824x

Reference yield: 25.0%

: 15243-33-1
dodecacarbonyl-triangulo-triruthenium

: 79133-89-4
diphenyl (2-thienyl)phosphine selenide

: [Ru3(μ3-Se)(μ-PPh2)(μ-η1:η2-C4H3S)(CO)6(P(C4H3S)(C6H5)2)]

: [Ru3(μ3-Se)2(CO)7(P(C4H3S)(C6H5)2)2]

Guidance literature:: With Me₃NO; In toluene; under N2, ruthenium cluster treated with (Ph2(C4H4S)PSe (1:2) and Me3NOin toluene for 2 h at 70°C, evapd. to dryness, dissolved in CH2Cl2; chromd. (silica, CH2Cl2/hexane=1:1), elem.anal.;
DOI:10.1016/S0020-1693(99)00547-2